Technology of production of powder and composite materials


Ministry of Education and Science of Republic of Kazakhstan

Karaganda State Technical University

 

 

 

Confirmed by

Chairman of the Academic Council,

rector, RK NAS academician

Gazaliyev A.M.

_______________________

_________ ____, 20___.

 

 

 

 

 

Syllabus

 

Course TPPCM 330  «Technology of production of powder and composite materials »

Module TPMP 32 « Technological processes  for materials production»

Major 5В071000 – «Materials Science and Technology of  New Materials”

Mechanical Engineering Institute

Department of Metallurgy, Materials Science and Nanotechnologies

 

 

 

 

2012

 Preface

 

Syllabus is worked out by cand. of Sc.,professor Zhukebayeva T.Zh., Senior tutor Atambayev J.N.

 

 

 

Discussed at the meeting of the department « Metallurgy, Materials Science and Nanotechnologies »

Minutes № _______ of ______________ «____» 20___

Head of department ________________    ___________«____» 20___

(signature)

 

 

Approved by the Educational Council of the Mechanical Engineering Institute

Minutes №  _______ of ______________ «____» 20___

Chairman  ________________        ____________ «____» 20___

(signature)

 

 

 


 

Tutor’s personal data and contact information

Cand. of  Sc., professor Ashkeyev Z.A..,  Senior Lecturer Atambayev J.N.

 

«Metallurgy, Materials Science and Nanotechnology» chair is in the main building of KSTU, B. Mira, 56 room No.313, contact phone 56-59-35 add.

1024Course labour intensity

Term

Number of credits /

ЕCTS

Type of classes

number of AL

Total number of hours

Forms of Control

Number of contact hours

number of OH

Total hours

lectures

Practical classes

Laboratory classes

6

3

30

15

45

90

45

135

Examination

 

 

Course description

Course “Theory and technology of production of powder and composite materials” is the higher education component of the cycle of basic disciplines. The course examines the major theoretical issues technologies for powder and composite materials, namely, properties, methods for producing powders items formed of powders, sintering processes, thermal, chemical, thermal and thermo-mechanical treatment, as well as the main trends in powder metallurgy the development of new metallic and composite materials. For successful completion of the course requires knowledge of subjects such as “Physical Materials”, “Physical properties of materials”, “Mechanical Properties of Materials”, “Physical and Colloid Chemistry”, “Theory and technology of heat treatment.”

 

Course purpose

The purpose of this course is to study the theoretical fundamentals of technology for powder and composite-traditional products to ensure the rational use of materials with regard to the technological and economic feasibility study of the properties and structure of materials, classification, labeling, and applications.

 

Course objectives

As a result of studying of this Course student:

student knows:

– structure and functions of metrological services;

– technical base of metrological ensuring production;

– methods of ensuring unity and accuracy of measurements;

– rules of metrological preparation and performance of testing works, processings and registrations of their results;

student is able:

– to analyze a condition of metrological ensuring production;

– to support in metrological working order of means of measurements and control;

– to develop techniques of checking of measuring instruments;

– to plan and carry out processes of measurements, tests and control;

– to process results of measurements;

– to define metrological characteristics of measuring instruments;

– to count errors in actual practice the organizations of works on metrological tests and to certification of gages.

Student is able to use results of innovative researches for performance of individual tasks.

 

Prerequisites

Studying of this course requires assimilation of  the following courses (with the indication of sections (subjects)):

 

Course

Name of sections (subjects)

1 Chemistry. Periodic table. Types of chemical bonds.
The kinetics of chemical reactions.
Diffusion processes. Fick’s laws.
Gibbs energy, Helmholtz energy
2 Physics. Solid State Physics.
Structure and physical properties of metals.
Electromagnetism.
Mechanics.
3 Mechanical properties of metals. Methods for determining the mechanical properties.
Units of different mechanical properties.
Types of defects in the crystal structure.
The influence of defects on the properties of the alloys.
4 Metrology, standardization and certification. Quality control.
State standards.

 

Post requisites

The knowledge gained in the study of the course Technology of production of powder and composite materials ” are used in the performance of the course project and the final work.

 

Thematic plan of course

Name of section (subject)

Labour intensity on types of classes

lectures

practical

laboratory

OH

AL

1. Subject and content of the course. Development of powder metallurgy. Chemical and physical properties of powders.

2

2

4

4

2 Technological properties of powders. Methods of producing metal powders: physical, chemical and mechanical.

4

2

4

4

3 The technology of three pieces. Shaping powder products molding. Rolling powders. Squeezing.

3

4

4

4

4 sintered pressed billets. Physico-chemical basis of the sintering process. Effect of temperature, time, environment sintering and pressing pressure on the sintering process. Sintering of single-component and multi-component powder blends. Sintering in the presence of a liquid phase.

4

4

4

5 Thermal and chemical-thermal treatment of powder products. The study of the structure of powder materials.

2

2

4

4

6 Structural powder materials, their classification. Strength and porosity of materials of construction. Basic principles of metal-ceramic production.

3

3

5

5

7 Composite Materials. Classification and properties of CM. Form filler: zero-dimensional, one-dimensional, two-dimensional.

3

5

5

8 Dispersion-toughened CM. Structure and properties. Technology for producing dispersion strengthened CM.

3

2

5

5

9 Fibre (reinforced) composites. Structure and properties. Technology for producing fibrous CM.

3

5

5

10 Methods of making fiber CM: solid and liquid phase. Precipitation and evaporation.

3

5

5

TOTAL:

30

15

45

45

 

Criteria of students’ knowledge assessment

The examination mark is determined by course as the sum of the maximum indexes of progress on midterm controls (to 60%) and to final attestation (examination) (to 40%) and makes value to 100% according to the table.

 

Grade on alphabetic system

Numerical

equivalents

Percentage

Traditional

system

А

А-

4,0

3,67

95-100

90-94

Excellent

В+

В

В-

3,33

3,0

2,67

85-89

80-84

75-79

Good

С+

С

С-

D+

D-

2,33

2,0

1,67

1,33

1,0

70-74

65-69

60-64

55-59

50-54

Satisfactory

F

0

0-49

Unsatisfactory

 

Grade «A» (excellent) is put in the case if student during a term showed perfect knowledge of all program questions of course, and also of subjects of independent work, regularly handed over midterm tasks, showed independence in studying of theoretical and applied questions according to the main program of studied course, and also on extra program questions.

Grade «A-» (excellent) stipulates perfect knowledge of basic laws and processes, concepts, ability to generalization of theoretical questions of course, regular handing of midterm tasks of classroom and independent work.

Grade  “B+” (good) is put in the case if student showed good and excellent knowledge of course questions, regularly handed over term tasks generally on “excellent” and some on “good”.

Grade “B” (good) is put in the case if student showed good knowledge of the questions opening the main maintenance of a concrete subject of course, and also subject of independent work, regularly handed over term tasks on “good” and “excellent”.

Grade “B-” (good) is put to a student in the case if he well is guided in theoretical and applied questions of course both on classroom, and on AL subjects, but irregularly handed over midterm tasks and had cases of a repeating an examination of term tasks on course.

Grade “C+” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “good” and “satisfactory” term tasks.

Grade “C” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “satisfactory” term tasks.

Grade “C-” (satisfactory) is put to a student in the case student during a term regularly handed over term tasks, but concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.

Grade “D+” (satisfactory) is put to a student in the case he irregularly handed over term tasks concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.

Grade “D-” (satisfactory) is put to a student in the case he irregularly handed over term tasks, concerning room classes and AL, owns the minimum volume of knowledge, and also allowed admissions of classes.

Grade “F” (unsatisfactorily) is put when student practically doesn’t own the minimum theoretical and practical material of room classes and AL on course, irregularly visits classes and doesn’t hand over in time term tasks

Midterm control is carried out on the 7, 14 weeks of study and it develops        proceeding from the following types of control:

 

Type of control

Percentage

Academic period of study, week

Total, %

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Attendance

0,7

*

*

*

*

*

*

*

*

*

*

*

*

*

*

10,0

Lectures notes

3,0

*

*

6,0

Test quiz

5,0

*

*

10,0

AL

1,0

*

*

*

*

*

*

*

*

*

*

*

*

*

*

14,0

Handing of course project 20,0

*

20,0
Examination

40

Total on    attestation

30

30

60

Total

100

 

Policy and procedures

At the studying course “Theory and technology of production of powder and composite materials” I ask to observe the following rules:

1. Not to be late for classes.

2. Not to miss classes without a good reason, in case of an illness I ask to submit the reference, in other cases – an explanatory note.

3. Duties of the student include visit of all types of classes.

4. According to the schedule diagram of educational process to hand over all types of control.

 

Educational and methodological provision of the discipline

Author

Literature

Publishing house, year of the issue

Number of copies

At

library

at department

Main literature

1. Cypresses S.S., G.A. Libenson Powder metallurgy. Moscow, Metallurgy, 1991. 432 p.

2

2. A.N. Stepanchuk et.al. Powder metallurgy. K.: Vyshcha School, 1989. 414 p.

4

3. Ed. Arzamasova B.N., Mukhina G.G. Materials science. Moscow: Publishing House of the MSTU. NE Bauman, 1986. 383 p.

17

3

4. Balbekova B.K Powder and composite materials.

Karaganda: KSTU, 2005. 81.

35

20

5. Balbekova B.K. Medvedev I.E., Zhashkeev E.K. Method. decree. to the lab. slave. the course “Technological bases Mfr. powder and composite materials “

Karaganda: KSTU, 2005. 47p.

6. Balbekova B.K.

Medvedev I.E.

Method. decree. IWST for the course “Technological principles of powder and composite materials.”

Karaganda, KSTU, 2007. 46.

35

7. B.N.Babich, E.V Vershinin, V.A Glebov, and others, ed. Yu.V. Levinskyi Metal powders and powder materials: a handbook.

М.: Ecomet, 2005. 520 с.

2

Additional literature

8. Andrievsky R.A. Powder Materials. Moscow: Metallurgiya, 1991. 208 p.

2

9. Libenson G.A. Processes of powder metallurgy. Moscow: MISA, V.1-2, 2002.

1

10. Antsiferov VN Bobrov GV Druzhinin LK etc. Powder metallurgy and sprayed coatings: A Textbook for high schools. Moscow: Metallurgiya, 1987. 792 p.

87

1

 

Schedule of performing and passing tasks on course

Type of control

Purpose and content of assignment

Recommended literature

Duration

Form of control

Handing term

Lab. work. № 1 Deepening knowledge on the subject.

[1, 5, 10]

2 week

Midterm

2-week

Report on the AL Deepening knowledge on the subject.

[1, 4, 7, 8]

1-3 week

Midterm

3- week

Lab. work. number 2 Deepening knowledge on the subject.

[1, 4, 5, 7]

4-6 week

Midterm

6- week

Report on the AL Deepening knowledge on the subject.

[1, 4, 10]

4 week

Midterm

4- week

C.W. № 1 Control of knowledge on topics 1-2.

[1,4-7, 10],

synopsis
lectures

1 week

Midterm

5- week

Lab. work. № 3 Deepening knowledge on the subject.

[1, 5, 10]

4 week Midterm 5- week
Report AL Deepening knowledge on the subject.

[1, 4, 6, 9]

2 week Midterm 6- week
Lab. work. № 4 Deepening knowledge on the subject.

[1, 5, 9]

2 week Midterm 7 week
Report AL Deepening knowledge on the subject.

[1, 3, 4, 9]

7-8 week Midterm 8-9 week
C.W. № 2 Control of knowledge on topics 3-4

[1, 4-6, 9],

synopsis
lectures

1 week Midterm 10 week
Lab. work. № 5 Deepening knowledge on the subject.

[1, 4, 5, 7]

4 week Midterm 11- week
Report AL Deepening knowledge on the subject. [1-4]         9 week Midterm 12- week
Lab. work. № 6 Deepening knowledge on the subject. [1, 5, 8]        2 week Midterm 12 week
Report on the AL Deepening knowledge on the subject. [1-4]        3 week Midterm 13 week
Lab. work. № 7 Deepening knowledge on the subject. [1-5]        4 week Midterm 14 week
C.W. № 3 Control of knowledge on topics 5-7

[1-4, 6, 9],

synopsis
lectures

1 week Midterm 14- week
abstract More detailed knowledge on the abstract

[1-5],

      periodical.

during a term

14- week
Examination Control of knowledge on the course The entire list of basic and additional literature

2  contact hours

Final During the session

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

State pub. lic. No.  50 of 31.03.2004 Passed for printing

Format 60х90/16

Printers sheets sh. Number of copies cop. Order  Contract price

__________________________________________________________________

Publishing house of Karaganda State Technical University

100027, Karaganda, Mira Boulevard, 56

 

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