Physical Materials Science

Ministry of Education and Science of Republic of Kazakhstan

Karaganda State Technical University

 

 

Confirmed by

Chairman of the Academic Council,

rector, RK NAS academician

Gazaliyev A.M.

_______________________

_________ ____, 20___.

 

 

Syllabus

 

 

Course PhMS 2209 « Physical Materials Science»

Module PhCPMS 20 « Physical Materials Science»

for students of major

5В073200 – Standardization, certification and metrology (on branches)

Institute of Mechanical engineering

Chair of Mechanical engineering technology

2013

Preface

 

Syllabus is worked out by cand. of eng., professor Sharaja O.A., senior tutor Platonova E.S.

 

 

 

Discussed at chair meeting «Mechanical engineering technology»

Minutes № _______ of ______________ «____» 20___

 

Head of chair ________________    ___________«____» 20___

(signature)

 

Approved by the Educational Consul of the Institute of Mechanical Engineering

Minutes №  _______ of ______________ «____» 20___

 

Chairman  ________________        ____________ «____» 20___

(signature)

 

 

Agreed with chair ____________________________________

                                                      (name of chair)

Head of chair _____________       ____________ «____» 20___

                                (signature)

Tutor’s personal data and contact information

cand. of eng., professor Sharaja O.A.

senior tutor Platonova E.S.

Chair MLP and KM is in the principal cage of KSTU (B.Mira, 56), auditory 313, the contact earphone 56-59-35доб. 1024.

 

 

Course labour intensity

Term	Number of credits / ЕCTS	Type of classes					number of AL hours	Total number of hours	Forms of Control
		Number of contact hours			number of ALT hours	Total hours
		lectures	Practical classes	Laboratory classes

 

4

3

15

15

15

45

90

45

135

Examination

 

Course characteristic

Course «Physical materials technology» is included cycle of the base disciplines studied at preparation of bachelors on trade 050710 «Materials technology and production engineering of new materials». The knowledge of the fundamentals of quantum mechanics, soli-state physics and the theory of phase changes of heading is necessary for understanding of structure of metal and nonmetallic materials, their properties, regularity of the phase changes occurring at deriving and machining of finished articles. The knowledge of the theoretical fundamentals allows scientifically obosnovanno to choose chemical compounds, regimes of manufacture, casting and machining of materials.

 

Course purpose

Course «Physical materials technology» sets as the purpose acquaintance with structure and properties of metal and nonmetallic materials, regularity of the phase changes occurring at thermal, chemistry-thermal and other processing methods. The gained knowledge is necessary for sampling of rational production engineering of deriving of preforms from various materials.

 

Course objectives

Course tasks the following: mastering by bachelors of regularity of change of physico-chemical and mechanical properties of materials depending on their phase composition and structure which are in turn shaped depending on their chemical compound and treatment schedules.

As a result of studying of this course:

student knows:

– about the theory of structure of materials;

– about structures of pure metals and solid solutions;

– about intermetallic bonds;

– about phase changes in solid;

– essence of phase changes and structural changes in metals;

– structure and properties of steels, powdered, composition and nemetal licheskih materials;

student is able:

– to analyse constitutional diagrams of double and threefold systems;;

– to apply the gained theoretical knowledge to processes weight materials;

– to acquire practical skills:

– thermodynamic justification of phase diagrams;

– conductings of experimental methods of probe of phase composition, structure, physico-chemical and mechanical properties of various materials.

 

Prerequisites

Studying of this course requires assimilation of the following courses (with the indication of sections (subjects)):

 

 

Post requisites

The knowledge gained at study of discipline «Physical materials technology», is used at mastering of following disciplines:

1.     The theory and high-heat treatment production engineering.

2.     Processes of manufacture of materials.

1. The scientific fundamentals of sampling of materials.
2. The theory of structure of materials.
3. The technological fundamentals of manufacture powdered and composite materials.
4. Mechanical properties of materials.
5. Physical properties of materials.

 

Thematic plan of course

 

 

List of laboratory classes

1. Electronic shell of atoms of chemical elements.

2. Thermodynamics of phase changes.

3. The assaying of glow irises of phase equilibrium of alloys.

4. Phase composition and structure of steel alloys.

5. The assaying of structure of alloys on the basis of non-ferrous metals.

 

 

Theme of course projects (works)

1 Device of metallographic microscope the MIME – 7.

2 Study of process of primary crystallization.

3 Study of the glow iris “iron-cement carbide” and microscopic structures of steels and white irons.

4 Study of microscopic structures and hardness became after hardening.

5 Microstructure analysis of heat-resistant steel.

6 Microstructure analysis latunej.

7 Definition of damp of nonmetallic materials.

8 Definition of brittleness temperature of rubbers at blow.

 

 

Thematic plan of office hours

OH theme	Objectives	Form classes	Contents of classes	Recommended literature
Subject 1. Electronic structure of atoms	Deepening of knowledge on the given theme	Problem solving	Problems on filling-up of electronic shells of atoms; definition of valence electrons	[3]
Subject 2. Thermodynamics of phase changes.	Deepening of knowledge on the given theme	Problem solving	Calculation of thermodynamic magnitudes of various processes	[6, 11]
Subject 3. Application of the theory of phase changes to concrete systems of alloys.	To learn to discriminate evtekticheskoe, evtektoidnoe, peritekticheskoe transformations	Problem solving	Construction of constitutional diagrams of two-component alloys with various phase changes	[2, 5, 7]
Subject 3. The theory of alloys.	To learn to define phase composition in points of the glow iris “iron-carbon”	Problem solving	Calculations by rule of bar (cuts): opre-division of density komponen in phases and quantitative relationship of phases	[2, 4, 8]
Subject 4. Crystallization of metals and alloys	Deepening of knowledge on the given theme	Operation with the glow iris “iron-CEMENT CARBIDE”	Refrigeration and heating up plotting	[4, 6, 7, 10]
Subject 5. Structure and methods of estimation of properties of metals and alloys	Deepening of knowledge on the given theme	Operation with the glow iris “iron-CEMENT CARBIDE”	Definition of temperatures of crystallization range of times-personal of alloys	[4, 6, 7, 10]
Subject 6. Deriving of articles by powder metallurgical techniques	Deepening of knowledge on the given theme	Problem solving	Definition of bulk tightness and tightness utrjaski, porosity, plasticity of dusts	[12]
Subject 7. The high-heat treatment fundamentals	Deepening of knowledge on the given theme	Operation with the glow iris “iron-CEMENT CARBIDE”	Assignment of regimes of hardening of various alloys	[2, 4, 6, 13]
Subject 8. Constructional and tool steel	Deepening of knowledge on the given theme	Operation with the literature	Definition of brands of steels	[2, 4, 10, 13]
Subject 9. Properties of materials	Deepening of knowledge of assignment of brands of steels and agency of alloying elements on properties of steels	Operation with marochnikami, the solution of problem of synthesis of alloy with demanded properties	Sampling of steel quality and alloying elements for deriving of necessary properties	[2, 13]
Subject 10. Non-ferrous metals and alloys	Deepening of knowledge on the given theme	Construction of the glow iris and the assaying	The aging process assaying on instance of glow iris Al–Cu	[2, 6, 10]
Subject 11. Study of structures of metals and alloys	Deepening of knowledge on the given theme	Operation with the literature	The assaying of structures of various alloys	[4, 6, 7, 10]
Subject 12. Circuit designs of reinforcement of composite materials	Deepening of knowledge on the given theme	Operation with the literature	Construction of circuit designs under the filler shape (null-dimensional, one-dimensional, two-dimensional) and KM with monoaxial, biaxial and trehosnym reinforcement	[2]
Subject 13. Plastic materials	Deepening of knowledge on the given theme	Calculation	Scaling of performances of slippage of plastic	[2, 4, 10]
Subject 14. Rezinotehnichesky articles	Deepening of knowledge on the given theme	Operation with the literature	Study of features of structure of rubbers (trans- and tsis – configurations)	[2, 10]
Subject 15. Glass, as material for mashino – and pribo-rostroenija	Deepening of knowledge on the given theme	Operation with the literature	The assaying of circuit designs for-tverdevanija glasses and chip	[2, 4]

Subjects of control tasks for AL

1 Individual jobs on preparation of abstracts.

2 Individual jobs by definition properties of materials.

 

 

Criteria of students’ knowledge assessment

The examination mark is determined by course as the sum of the maximum indexes of progress on midterm controls (to 60%) and to final attestation (examination) (to 40%) and makes value to 100% according to the table.

 

 

Mark «A» (excellent) is put in the case if student during a term showed perfect knowledge of all program questions of course, and also of subjects of independent work, regularly handed over midterm tasks, showed independence in studying of theoretical and applied questions according to the main program of studied course, and also on extra program questions.

Mark «A-» (excellent) stipulates perfect knowledge of basic laws and processes, concepts, ability to generalization of theoretical questions of course, regular handing of midterm tasks of classroom and independent work.

Mark “B+” (good) is put in the case if student showed good and excellent knowledge of course questions, regularly handed over term tasks generally on “excellent” and some on “good”.

Mark “B” (good) is put in the case if student showed good knowledge of the questions opening the main maintenance of a concrete subject of course, and also subject of independent work, regularly handed over term tasks on “good” and “excellent”.

Mark “B-” (good) is put to a student in the case if he well is guided in theoretical and applied questions of course both on classroom, and on AL subjects, but irregularly handed over midterm tasks and had cases of a repeating an examination of term tasks on course.

Mark “C+” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “good” and “satisfactory” term tasks.

Mark “C” (satisfactory) is put to a student in the case he owns questions of conceptual character by all types of room classes and AL, can open the maintenance of separate modules of course, hands over on “satisfactory” term tasks.

Mark “C-” (satisfactory) is put to a student in the case student during a term regularly handed over term tasks, but concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.

Mark “D+” (satisfactory) is put to a student in the case he irregularly handed over term tasks concerning room classes and AL owns only the general concepts and can explain only separate regularities and their understanding within a concrete subject.

Mark “D -” (satisfactory) is put to a student in the case he irregularly handed over term tasks, concerning room classes and AL, owns the minimum volume of knowledge, and also allowed admissions of classes.

Mark “F” (unsatisfactorily) is put when student practically doesn’t own the minimum theoretical and practical material of room classes and AL on course, irregularly visits classes and doesn’t hand over in time term tasks.

Midterm control is carried out on the 7, 14 weeks of study and it develops proceeding from the following types of control:

 

Policy and procedures

At discipline study «Physical materials technology» I ask to observe following rules:

1. Not to be late for holdings.

2. Not to pass holding without good reason, in case of sickness I ask to present the inquiry, in other cases – explanatory note.

3. Duties of the student include visiting of all aspects of holdings.

4. According to the schedule of educational process to return all aspects of control.

5 Let pass practical and laboratory researches to complete in the time specified by the teacher.

6. To disconnect cellular telephones during holdings, to keep quiet and order.

7. Actively to participate in educational process.

8. To be tolerant, opened, frank and benevolent to fellow students and teachers.

 

Educational and methodical provision of course

Author	Literature	Publishing house, year of the issue	Number of copies
			in library	at department
1	2	3	4	5
Main literature
1. Caen of River U, Haazen of the Item	Physical metal science.	Metallurgy, 1987	15	2
2. Arzamasov B. N, Makarova V. I, Mukhin G. G, etc.	Materials technology.	M: MGTU of Bauman, 2001.	5	–
3. Isin D.K., Isagulov A.Z.	Soli-state physics.	Karaganda: izd. KSTU, 2005	–	1
4. Lahtin J.M., Leonteva of Century of the Item	Materials technology.	M: Engineering industry, 1990.	6	1
5. Zaharov A.M.	Constitutional diagrams of double and threefold systems.	M: Metallurgy, 1978.	1	2
6. Livshits B.	Microscopic metallography.	M: Metallurgy, 1990.	1	–
7. Sharaja O. A, Balbekova B. K.	Method. The decree. To prakt. zan. At the rate «Tehnologich. Process. mash. proizv.: Materials technology».	Karaganda: izd. KSTU, 2005г.	5	1
8. Smolkin A.A., Isagulov A.Z., Sharaja O. A.	Method. The decree. «The mat-rialovedenie. Labo-ratornyj expert.»	Karaganda: izd. KSTU, 1997г.	1	–
Additional literature
Ahiezer A.I.	Atomic physics	Kiev: Naukova dumka, 1988	1	1
Mozberg R. K.	Materials technology.	M: the Higher school, 1991.	1	1
Koroticha V. I.	Metallurgy	Sverdlovsk: Uralsk. gos. tehn. Un y, 2001	1	–
Kiparisov S.S., Libenson G. A.	Powder metallurgy.	M: Metallurgy, 1991.	10	50
Pinchuk of h.p., etc.	Materials technology and structural materials.	Minsk, the Higher school, 1989.	10	50
Balbekova B. K, Tulegenova S.N., Malashkevichute E.O., Medvedeva I.E.	Method. The decree. To lab. The slave. On dists. «Me-tallovedenie color. Threw.».	Karaganda: izd. KSTU, 2005.	–	1

 

 

 

Schedule of performing and handing in assignments on course

Type of control	Purpose and content of assignment	Recommended literature	Duration	Form of control	Handing term
1	2	3	4	5	6
Problem solving on prakt. It is occupied. 1	To deepen knowledge on electronic structure of elements of Periodicheskoj tablitsa D.I.	[1-2]	2 weeks	current	2 week
Execution lab. The slave. 1	To familiarize with the light microscope device	[8]	2 weeks	current	2 week
The record on AL (themes 1,2)	To deepen knowledge on the passed material	[1-4, 9-10]	1-3 weeks	current	3 week
Execution lab. The slave. 2	To familiarize with process of primary crystallization of metals	[8]	2 weeks	current	3 week
Analysis of questions on prakt. занят.2	To deepen knowledge on theme «the Thermodyne-mika in metallove-denii»	[2, 6]	2 weeks	current	4 week
Execution lab. The slave. 3	Study of the glow iris “iron-CEMENT CARBIDE” And microscopic structures of steels and white irons	[8]	3 weeks	current	5 week
K.R. № 1	Attaching and control of knowledge on the passed themes 1-4	[1-4, 6], the abstract of lectures	1 week	current	5 week
The record on AL (themes 3,4)	To deepen knowledge on the passed material	[2, 4, 6]	1-3 weeks	current	5 week
Problem solving on prakt. занят.3	To deepen knowledge on theme «Phase diagrams of two- and three-component systems»	[11]	2 weeks	current	6 week
Execution lab. The slave. 4	Study of microscopic structures and hardness of steel After hardening	[8]	2 weeks	midterm	7 week
The record on AL (themes 5)	To deepen knowledge on the passed material	[6, 7, 11]	1-3 weeks	midterm	7 week
Execution lab. The slave. 5	Microstructure analysis of heat-resistant steel	[2, 6, 8]	2 weeks	current	8 week
Problem solving on prakt. занят.4	To deepen knowledge on theme «Phase composition and structure of steel alloys»	[2, 5-8]	8 weeks	current	12 week
K.R. № 2	Control of knowledge on themes 5-9	[2-7, 10, 11], the abstract of lectures	2 weeks	current	10 week
The record on AL (those ow 6, 7, 8, 9, 10)	To deepen knowledge on the passed themes	[2-7, 10, 11]	5 weeks	current	11 week
Problem solving on prakt. занят.5	To deepen knowledge on theme «Alloys on the basis of non-ferrous metals»	[6, 12]	2 weeks	current	14 week
Execution lab. The slave. 6	Microstructure analysis latunej	[2, 11, 12]	1 week	current	10 week
The record on AL (themes 11, 12,13)	To deepen knowledge on the passed themes	[1, 2, 6, 7]	1-3 weeks	midterm	14 week
Execution lab. The slave. 7	Definition of damp of nonmetallic materials	[2, 11, 12]	1 week	midterm	14 week
The record on AL (themes 14, 15)	To deepen knowledge on the passed material	[2, 4, 10]	2 weeks	midterm	14 week
Execution lab. The slave. 8	Definition of brittleness temperature of rubbers at blow	[2, 11, 12]	1 week	current	15 week
K.R. № 3	Control of knowledge on themes 14, 15	[2, 4, 10], the abstract of lectures	2 weeks	current	15th week
The abstract	Deepening of knowledge on abstract theme	[1,2,6,7], the period. izd.	During semester	current	15th week
Examination	Check of assimilation of material of discipline	All list of the basic and additional literature	2 contact hours	final	In session

 

Questions for self-checking

1. What circle of questions studies physical materials technology?

2. What link of physical materials technology with other branches of science and engineering?

3. On what groups probe methods in physical materials technology share?

4. What methods of probe refer to to the experimental?

5. What experimental methods refer to to straight lines, and what microstructure analyses to indirect methods and microscopic structures?

6. How the space near to kernel in which the probability of finding elektrona is great enough is called?

7. How it is possible to present condition elektrona in atom?

8. What is the energy level?

9. What quantum number defines energy level?

10. What is the orbit quantum number characterized?

11. What defines magnetic quantum number?

12. What characterizes spin quantum number?

13. What values can accept each of quantum numbers?

14. In what the Pauli-Fermi principle consists?

15. In what the rule of Hunda consists?

16. What is the ionization potential?

17. How the potential of ionization of chemical elements of the table of D.I.Mendeleyev varies?

18. What metals are called as simple, what transitive?

19. Describe lanthanides and aktinoidy.

20. What types of crystal lattices are characteristic for metals?

21. What bonding force can be in metals?

22. Describe each type of bonding force in metals (ion, kovalentnuju, Van-der-Vaalsovu, metal).

23. What process is called as crystallization?

24. In what essence of homogeneous formation of germs?

25. In what essence of heterogeneous formation of germs?

26. What is the super-cooling extent?

27. Describe gears of growth of chips.

28. What factors influence the shape of chips?

29. The steel ingot consists of what zones?

30. How admixtures in bullion are arranged?

31. Describe polymorphic transformation.

32. What crystallographic link between new and old phases at phase changes?

33. Make definition of elastic and plastic strains.

34. Describe various aspects of voltage.

35. What essence of shear strain and twinning.

36. What name structure of strain and how it influences properties of metal?

37. Than the reinforcement of metal in the course of flowage speaks?

38. What fathom retrace process?

39. What is poligonizatsija?

40. What factors influence temperature process of recrtstallization?

41. What factors influence structure of recrtstallization?

42. In what cases the recrtstallization structure is advisable, and when it should be avoided?

43. What strain name cold, hot?

44. Make definition solid solution.

45. You know what types of solid solutions?

46. Enumerate the factors defining solid solubility.

47. What joints are called as intermetallic?

48. What joints are called as electronic joints?

49. What processes are called as thermochemical?

50. Make definition of enthalpy, entropy, energy of Gibbsa.

51. What magnitude characterizes equilibrium in responses between solutes?

52. In what the phase rule of Gibbsa consists?

53. What means concept “nonvariantnost”?

54. Give definitions evtekticheskim, evtektoidnym and peritekticheskim to transformations.

55. Make self-diffusion definition.

56. What means electro- and thermomigration?

57. How there is solidification of polyphase alloys?

58. In what essence of process of inoculation?

59. What transformation is called as the martensitic?

60. What alloys name metal glasses?

61. In what the essence of solid-phase sintering consists?

62. In what the essence of liquid-phase sintering consists?

63. Describe process of elevated-temperature compaction of powdered material.

64. What display S-shaped glow irises?

65. In what essence of dispersion hardening ferritnoj steels?

66. Describe rapid tool steels.

67. In what anomalous friability of steel consists?

68. What steels name doped?

69. What role of alloying elements in steels?

70. In what thermomechanical machining of steel consists?

71. What materials are called as aggregates?

72. How classify composite materials?

73. Properties of aggregates depend on what factors?

74. Where composite materials are applied?

75. What materials are called as plastic, what their classification?

76. Enumerate the major thermoplastic masses applied in engineering industry.

77. What serves as initial raw materials at deriving rezinotehnicheskih articles?

78. What equipment apply to deriving of rubbers?

79. Film materials and their variety.

80. Describe paintwork materials.